Information on the most widely used ASTM standards within the materials testing industry
ISO 11502 Standard | Blocking Resistance Test Machine for Plastic Film & Sheeting | UnitedTest
UnitedTest manufactures ISO 11502 compliant blocking testers for flexible plastic packaging factories and material testing labs worldwide.
ISO 11502 Plastics, Film and Sheeting – Determination of Blocking Resistance assesses blocking resistance, describing how easily stacked flexible plastic films or sheets self-adhere under combined heat and compression loads. The standard specifies two separate test protocols for full performance evaluation: qualitative Method A and quantitative Method B.
Our blocking test equipment supports both ISO 11502 test methods, delivering consistent qualitative judgment and quantitative blocking force data for film formulation R&D and production quality control.
Two Specific Test Methods
Method A: Qualitative Visual Screening Method
A rapid pass/fail assessment to judge whether blocking occurs after accelerated aging, without numerical force data.
After 24 h thermal compression aging at 50 °C / 7 kPa pressure, film pairs are manually peeled. Blocking is confirmed if:
A reference metal weight is lifted during separation; OR
Visible surface damage (transfer, peeling, scuffing) appears on film contact surfaces.
Method B: Quantitative Force Measurement Method
Measures the exact separation force (in Newtons) required to pull apart pre-aged stuck film layers using a universal tensile tester, delivering quantifiable blocking resistance values for performance comparison.
After 3 h accelerated aging at 50 °C / 3 kPa pressure, blocked film pairs are fixed to 100×100 mm aluminum platens on a tensile machine. The machine pulls the platens apart at a constant crosshead speed, recording the maximum tensile force needed to fully separate the two film layers as the quantitative blocking resistance value.
Test Specimen Specifications
Shared Specimen Dimensions
All test strips are cut to 150 mm (length) × 76 mm (width); long side aligns with the film machine direction (MD) for Method B.
Specimen Quantity
Method A: 6 total specimens, assembled into 3 test assemblies (face-face, back-back, back-face contact orientations)
Method B: 10 specimens, assembled into 5 identical test assemblies (uniform surface contact orientation selected by the user)
Required Test Equipment of ISO 11502 Plastics Film and lamination blocking resistance test:
For method B | Constant-speed Universal Testing Machine (UTM), Pair of matched 100 mm × 100 mm square aluminum platens with rigid UTM adapters 2.3 kg dead weight (creates 3 kPa aging pressure) Spatula/wide knife for careful specimen transfer |
| For method A | 5.4 kg dead weight (creates 7 kPa uniform pressure) 50 g and 100 g rectangular metal bars (separation weight indicators) Long-arm metal clip for manual film peeling Horizontal flat test bench surface |
| Auxiliary Equipment for A & B | Temperature-controlled oven (50 ±2 °C uniform heating) 100 mm × 76 mm glass plates (~2 mm thickness) 100 mm × 76 mm filter paper strips Double-sided pressure-sensitive adhesive tape Standard climate chamber for pre-conditioning per ISO 291. |
Key Test Parameters & Mandatory Stipulations:
| Parameter | Method A (Qualitative) | Method B (Quantitative) |
|---|---|---|
| Oven temperature | 50 ±2 °C | 50 ±2 °C |
| Compressive pressure | 7 kPa (5.4 kg weight) | 3 kPa (2.3 kg weight) |
| Aging duration | 24 hours | 3 hours |
| Post-aging recovery time | 2–24 h at standard atmosphere | 2–24 h at standard atmosphere |
| Method A manual peeling speed: 25 ±2.5 mm/s uniform manual pull rate Method B UTM crosshead speed: 5 mm/min constant separation speed. Surface Contact Configurations: Three standard contact combinations for printed films: face-to-face, back-to-back, back-to-face; all orientations must be tested for complete qualitative evaluation. | ||
Step by step Test Procedure of ISO 11502 Plastics Film and lamination blocking resistance test
Procedure A (Qualitative Method)
Condition specimens, glass plates and filter paper for 24 h per ISO 291.
Build three separate stacked assemblies with alternating glass plate, filter paper, two film specimens, filter paper, glass plate; each assembly uses one unique surface contact pairing. Leave 50 mm film overhang for easy peeling.
Load each assembly with 5.4 kg weight, place in 50 °C oven for 24 h aging.
Remove weights, cool assemblies for 2–24 h at standard atmosphere.
Separate film pairs, mount 50 g bar under unprinted films or 100 g bar under printed films.
Manually pull upper film at 25 mm/s; record if the metal bar lifts and check for surface damage.
Record blocking occurrence and surface defects for the test report.
Procedure B (Quantitative Method)
Pre-condition all test materials for 24 h under ISO 291 standard atmosphere.
Prepare five identical aging assemblies with glass plates, filter paper and paired film specimens; apply uniform surface contact orientation across all sets.
Load each assembly with 2.3 kg weight, heat at 50 °C for 3 hours.
Remove weights, cool assemblies for 2–24 h at standard conditions.
Transfer one blocked film pair symmetrically onto the lower aluminum platen of the UTM.
Lower the upper platen to rest flat on the film; peel back overhanging film edges with a knife.
Secure upper film ends to top platen and lower film ends to bottom platen with double-sided tape.
Set UTM crosshead speed to 5 mm/min, start test and record maximum separation force.
Repeat for all five assemblies, calculate average peak force as final blocking resistance.
Industrial Application Fields
ISO 11502 is a global standard widely adopted across international plastic film manufacturing and converting sectors:
Flexible food packaging: BOPP, PE, PET, CPP wrapping films, stretch/shrink wrap, laminated barrier films
Printing & coating industry: Printed decorative films, metallized packaging films, ink-coated substrates
Agricultural plastics: Greenhouse mulch film, crop silage wrap, large rolled agricultural sheeting
Medical packaging: Sterile flexible barrier films, disposable medical packaging rolls
Industrial protective films: Surface release films, optical plastic sheets, roll stock protective coverings
Consumer goods films: Household cling wrap, plastic bag stock, decorative printed films
Typical use cases: incoming raw material QC, anti-blocking slip agent formulation R&D, cross-border supplier quality acceptance, product shelf-life aging simulation, and comparative performance testing of different film grades.
Related Test Standard:
| ASTM D3354 | Standard Test Method for Blocking Load of Plastic Film by the Parallel Plate Method |
| ISO 11502 | Plastics - Film and lamination - Determination of blocking resistance |
| GB/T 39935 | Plastics—Film and sheeting—Determination of blocking resistance |
ISO 11502 vs ASTM D3354 — At a Glance
| Feature | ISO 11502 (Method B) | ASTM D3354 |
|---|---|---|
| Approach | Induces blocking (oven, 50°C, pressure) | Tests already blockedas-cut specimen |
| Induction | 3 kPa, 3 h, 50 °C | None |
| Contact area | 100×100 mm (implied by block size) | 100 cm² (explicit) |
| Speed | 5 mm/min crosshead | 5.1 mm/min (Proc B) or 90 g/min (Proc A) |
| Unit | N | g (max 200 g) |
| Precision | Not known (no interlab data yet per 5.5) | Known (Table 1, 6-lab round robin) |
| Qualitative option | ✅ Method A | ❌ |
| Printed film oriented | ✅ Explicit face/back | Not explicit |
Keywords: UnitedTest ISO 11502 blocking resistance tester, ISO 11502 plastic film blocking test machine, flexible sheeting heat-pressure sticking testing equipment, ISO 11502 qualitative Method A quantitative Method B blocking tester, stacked plastic sheet adhesion resistance inspection bench
Related products and device
Related Standard
ASTM D3354 Standard Test Method for Blocking Load of Plastic Film by the Parallel Plate Method
ASTM D3354 defines a parallel plate test to quantitatively measure blocking load—the unwanted adhesion force between stacked plastic film layers, reported in grams for a fixed 100 cm² contact area. Blocking refers to self-sticking of smooth film surfaces when air is fully excluded during rolling, storage or processing, worsened by heat and compression. The test only quantifies existing adhesion strength, not a material’s inherent tendency to develop blocking over time, with a maximum measurable load limit of 200g.
ISO 6383-2 Plastics — Film and sheeting — Determination of tear resistance — Part 2: Elmendorf method
ISO 6383-2 specifies the Elmendorf pendulum method to measure the force required to propagate an existing pre-cut slit across thin flexible plastic film and sheeting under standardized loading conditions.
ASTM D1204 Standard Test Method for Linear Dimensional Changes of Nonrigid Thermoplastic Sheeting or Film at Elevated Temperature
ASTM D1204 is method to measure linear dimensional change (shrinkage or expansion) of nonrigid thermoplastic sheeting/film when exposed to a specified elevated temperature and time in air. Applies to nonrigid thermoplastic sheeting/film made by calender or extrusion processes, the heating medium is air (mechanical convection oven) — this points is the fundamental difference from ASTM D2732 (liquid bath).
ISO 527-3 Plastics - TENSILE PROPERTIES - PART 3: FOR FILMS AND SHEETS
ISO 527-3 specifies the test conditions for determining the tensile properties of plastic films and sheets with a thickness less than 1 mm, based on the general principles of ISO 527-1. Provides standardized procedures to measure critical mechanical parameters including tensile strength, yield strength, elongation at break, and Young's modulus for thin plastic materials. It is critically important because thin films behave very differently under stress compared to rigid plastics; they are more prone to tearing, slipping, and deformation. By standardizing the test conditions, this document ensures that material specifications, quality control, and research data are globally comparable and reliable. Specimen created following ISO 527-3 can be used to determine the tensile properties of thin plastic sheets and films including the tensile modulus of elasticity and the tensile energy to break (TEB).
ISO 304:1985 Surface active agents — Determination of surface tension by drawing up liquid films
The maximum force is measured which is necessary to act vertically on a stirrup or a ring, in contact with the surface of the liquid being examined placed in a measuring cup, in order to separate it from this surface, or on a plate with an edge in contact with the surface, in order to draw up the film that has formed. The surface tension of pure liquids or other solutions can also be measured by this method.
ASTM D1922: Standard Test Method for Propagation Tear Resistance of Plastic Film and Thin Sheeting by Pendulum Method.
ASTM D1922 defines a laboratory method to measure the average force required to propagate (continue) a tear through a plastic film or non-rigid thin sheeting, after the tear has already been started. The test uses an Elmendorf-type pendulum tearing tester. It is applicable to plastic film (arbitrarily defined as sheeting ≤ 0.25 mm / 0.010 in.) and thin non-rigid sheeting, and is equivalent to ISO 6383-2.
ASTM D1004: Standard Test Method for Tear Resistance (Graves Tear) of Plastic Film and Sheeting
ASTM D1004 is a test method that determines the tear strength of flexible plastic film and sheeting at very low rates of loading using a constant-rate-of crosshead-movement type tensile testing machine. Tearing is produced in a small area of stress concentration of the plastic film or sheeting specimen at controlled speeds below the rate encountered in real world applications in order to produce the most reliable data, which can be used to compare and analyze the tear resistance. Actual use of performance in tearing of certain plastics may not necessarily corralate with the data acquired from this test method. The specimen geometry of this test method produces a stress concentration in a small area of the specimen. The maximum stress, usually found near the onset of tearing, is recorded as the tear resistance in newtons (or pounds-force). The method is not applicable for film or sheeting material where brittle failures occur during testing or where maximum extension is greater than 101.6 mm (4 in.).
FAQs for ISO 11502 Plastics – Film and Sheeting – Determination of Blocking Resistance
Q1: What is blocking as defined in ISO 11502, and what two test methods does this standard provide?
A: Blocking means unintended adhesion between two plastic film or sheet surfaces when they are tightly stacked. ISO 11502:2018 includes two independent test methods:
Method A: Qualitative screening method for simple pass/fail judgment of blocking severity without numerical force data.
Method B: Quantitative tensile method that measures the exact separation force (in Newtons) required to pull apart adhered film layers.
Q2: What is the core difference between ISO 11502 Method A and Method B?
A: Purpose: Method A is a fast qualitative check; Method B generates quantitative force values for performance comparison.
Aging parameters: Method A uses 7 kPa pressure for 24 h aging; Method B uses milder 3 kPa pressure for only 3 h aging.
Testing operation: Method A relies on manual peeling with reference metal bars to judge blocking; Method B uses a universal tensile tester to record maximum separation force.
Specimen quantity: Method A needs 6 specimens (3 assemblies of different surface contact pairs); Method B needs 10 specimens (5 identical assemblies for averaging).
Output result: Method A records only visual blocking phenomenon and surface damage; Method B outputs average peak separation force in Newtons.
Q3: Why is ISO 11502 different from ASTM D3354 even though both test film blocking? Can test results be interchanged?
A: They are similar but technically non-equivalent, so results cannot be directly compared or converted:
Pre-blocking aging: ISO 11502 artificially creates blocking via controlled heat + pressure aging; ASTM D3354 tests existing natural blocking without pre-aging treatment.
Specimen size, contact area, pressure and aging time are completely different.
Units: ISO 11502 Method B uses Newtons; ASTM D3354 uses grams.
ASTM D3354 has a maximum test load limit of 200 g, while ISO 11502 has no upper force limit.
ISO provides both qualitative and quantitative options; ASTM D3354 only has two quantitative tensile procedures.
Q4: What size are ISO 11502 test specimens, and what sampling rules must be followed?
A: Specimen dimension: 150 mm × 76 mm strips; long side aligns with film machine direction for Method B.
Sampling requirements: Cut samples at least 100 mm away from roll edges and over 1 m from the start/end of the film roll.
Resting rule: Films must sit for a minimum of 16 h after manufacturing before testing.
Printed films: Collect specimens covering all print colour combinations to test all possible contact surface pairs.
Q5: When does ISO 11502 confirm that blocking has occurred in Method A (qualitative test)?
A: Blocking is confirmed if either condition happens during manual separation:
The reference metal bar (50 g for unprinted film, 100 g for printed film) is lifted off the flat horizontal surface when peeling the film layers;
Visible surface damage, ink transfer, scuffing or material tearing appears on the contact sides of the film.
Q6: Why is ISO 11502 an important standard for plastic film manufacturers and global converters?
A: Simulates real storage conditions: Accelerated heat-pressure aging replicates long-term stacked roll storage and transport environments to predict blocking failures in advance.
Dual testing options for different QC needs: Fast low-cost qualitative screening for daily batch inspection; quantitative force data for formulation R&D and supplier qualification.
Global unified standard: As an ISO international standard, it harmonizes test methods across all countries, reducing trade disputes for cross-border film supply chains.
Guides anti-blocking formulation development: Quantitative force data helps optimize slip agents, anti-block masterbatches and extrusion processes to reduce adhesion without sacrificing other film properties.
Prevents costly production downtime: Severe blocking causes film tearing, unwinding jams and waste on printing, lamination and packaging machines; test results filter unqualified film batches before processing.
Complete evaluation for printed films: Special requirements for multi-colour printed specimens avoid overlooking ink-induced blocking or surface transfer defects.
Q7: How many replicate assemblies are required for Method B quantitative testing, and how is the final result calculated?
A: Five separate aging assemblies are prepared and tested individually. The maximum separation force (Newtons) of each replicate is recorded, and the average value of the five results is taken as the final blocking resistance of the material.
Q8: Why do we need a 2–24 h recovery period after oven aging before testing separation?
A: This cooling recovery step stabilizes the film’s temperature and internal stress after high-temperature aging, eliminating thermal expansion interference and ensuring consistent, repeatable separation force results.
Q9: What tools are used to judge blocking severity in Method A qualitative testing?
A: Two standard rectangular metal bars: 50 g for unprinted smooth film surfaces and 100 g for printed or ink-coated film surfaces. If the film’s adhesion can lift the bar, blocking is deemed significant.
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