Information on the most widely used ASTM standards within the materials testing industry
ASTM C1135 Structural Sealant Tensile Adhesion Tester | UnitedTest
UnitedTest manufactures high-precision ASTM C1135 compliant tensile testing instruments tailored to evaluate tensile adhesion performance of structural sealants for architectural structural glazing laboratories and sealant production quality control.
ASTM C1135 Standard Test Method for Determining Tensile Adhesion Properties of Structural Sealants outlines a standardized test procedure to analyze tensile stress and elongation characteristics of structural sealants bonded between two rigid substrate panels. This test setup accurately simulates the real stress conditions of structural glazing joints, where sealants serve as critical structural connectors between glass panels and metal framing systems.
During testing, the equipment captures multiple vital performance indicators: tensile adhesion performance, tensile stress at various elongation levels, ultimate tensile strength, and distinct failure modes of structural sealants. The comprehensive test data supports sealant formula optimization, curtain wall structural design validation, incoming raw material inspection, and finished structural glazing sealant certification.
Core Test Principle
The test is based on a tensile-to-failure configuration using an H-shaped ("H-specimen") geometry:
Two rigid substrate panels (default: clear float glass) are positioned parallel to each other, separated by a 12.7 mm × 12.7 mm × 50.8 mm sealant cavity
The structural sealant is applied to fill this cavity, forming two substrate/sealant interfaces
After a 21-day cure, the specimen is mounted in a tensile testing machine
A tensile load is applied perpendicular to the substrate/sealant interfaces at a constant rate of 50.8 mm/min
The tensile load is recorded at 10%, 25%, 50%, and 100% strain, and the percent strain at peak load is captured
The measured load is divided by the actual sealant contact area to calculate tensile stress at each strain level
The mode of failure (percent cohesive failure) is observed and recorded
Key principle: The H-shaped specimen geometry mimics actual structural glazing joint geometry — the sealant is adhered on two parallel faces and loaded in pure tension, eliminating the peel/bending stresses present in lap-shear configurations. This makes ASTM C1135 data directly relevant to structural glazing design.
Test Equipment required of ASTM C1135 Tensile Adhesion Test for Structural Sealants:
| Universal Tensile testing machine | Dual movable/fixed crosshead design with self-aligning swivel universal joint grips to eliminate eccentric off-axis loading Fixed crosshead travel rate: 50.8 mm/min (2.0 in/min) ±5.1 mm/min tolerance Chart recorder or digital data logger; minimum chart speed 127 mm/min (5.0 in/min), preferred 508 mm/min for precise strain load readings Fixture set to securely hold substrate panels without clamping the sealant zone |
| Specimen Fabrication Materials | Standard Substrates: Clear float glass panels (6.3 mm thickness ×25.4 mm width ×76.2 mm length). Metal/aluminum substrates permitted if rigidity is verified. PTFE (Teflon) one-piece solid spacer: Non-stick material to form precise rectangular sealant cavity with zero adhesion to sealant. Application tools: Caulking gun, flat spatula for filling and trimming sealant flush with spacer surfaces Substrate cleaning supplies: 50/50 isopropanol-water mixture (standard cleaning solvent per precision data report) + lint-free dry cloths. |
| Measuring Tools | Precision caliper accurate to 0.01 mm to measure actual sealant bond length (A) and edge bite width (B) for contact area calculation. |
Test Specimen Information:
| Sealant cavity (Length × Width × Depth) | 12.7 mm × 12.7 mm × 50.8 mm (0.50 in. × 0.50 in. × 2.0 in.) |
| Dimension A (sealant length) | Measured to nearest 0.8 mm |
| Dimension B (sealant bite / contact depth) | Measured to nearest 0.8 mm |
| Substrate size (default) | 6.3 mm × 25.4 mm × 76.2 mm clear float glass |
| Number of specimens per condition | 5 |
Substrates wiped with clean, dry, lint-free cloth, then cleaned with appropriate solution (50/50 isopropanol/water for glass), wiped dry before solution evaporates;
Sealant filled completely into cavity; surface tooled to ensure complete filling and wetting of substrate surfaces; struck off flush with substrate
Five specimens assembled per sealant/substrate combination
An additional set of 5 specimens required for each additional environmental condition being evaluated.
Test Parameters & Stipulations
| Parameter | Value |
|---|---|
| Tensile rate | 50.8 ± 5.1 mm/min (2.0 ± 0.20 in./min) |
| Chart speed (if analog recording) | Minimum 127 mm/min (5.0 in./min); 508 mm/min (20.0 in./min) preferred |
| Curing period | 21 days at standard conditions |
| Standard conditions | Per ASTM C717 (typically 23°C ± 2°C, 50% ± 5% RH) |
| Specimens per condition | 5 (plus 5 per additional environmental condition) |
| Sealant cavity | 12.7 mm × 12.7 mm × 50.8 mm |
| Strain recording points | 10%, 25%, 50%, 100%, and peak load |
| Measurement accuracy | Dimensions A and B to nearest 0.8 mm (0.03125 in.) |
21-day cure — At standard conditions; deviations must be reported
Spacer removal — All spacers removed before testing (early removal allowed with notation)
Test Procedures for ASTM C1135 Tensile Adhesion Test for Structural Sealants
Step 1 Specimen Fabrication & Cure
Clean glass substrates, apply primer as needed, assemble PTFE spacer mold, fill sealant without trapped air bubbles, trim surfaces flat, cure 21 days under standard ambient atmosphere. Remove spacers before testing (record early removal if done).
Step 2 Pre-Measure Bond Dimensions
Use precision calipers to measure actual sealant bond length (A) and edge bite width (B) for each coupon; calculate individual contact area D = A × B. Record any visible internal air bubbles in sealant bulk.
Step 3 Tensile Machine Setup
Mount swivel self-aligning fixtures into upper/lower grips, set crosshead speed to 50.8 mm/min, activate chart recorder at minimum 127 mm/min speed.
Step 4 Mount Specimen
Clamp glass substrate ends into machine fixtures; ensure tensile load acts perpendicular to the sealant-substrate bonded plane with no eccentric twisting.
Step 5 Tensile Loading to Rupture
Initiate crosshead travel; continuously record tensile load values at 10%, 25%, 50%, 100% strain and peak ultimate load until full specimen separation. If glass substrate breaks mid-test, discard rupture load but retain all pre-break strain data.
Step 6 Post-Test Failure Classification
Visually inspect fractured surfaces, calculate percentage of cohesive failure (crack inside sealant) versus adhesive interfacial detachment; document all test anomalies (bubbles, substrate fracture, uneven bonding).
Step 7 Data Reduction
Calculate tensile stress (MPa/psi) at each specified elongation point and ultimate tensile strength for every replicate; compute average values across 5 specimens.
Industry Application Fields
ASTM C1135 is used in industries where structural sealants provide the primary load-bearing connection between glazing/panels and framing systems:
| Industry / Sector | Applications |
|---|---|
| Structural Glazing (Curtain Walls) | The primary application — evaluating structural silicones that bond glass lites to metal frames in curtain wall systems. The H-specimen geometry directly replicates the joint configuration. |
| Architectural Glazing | Structural bonding of glass panels, spandrel panels, and decorative glazing elements to aluminum/steel frames |
| Insulating Glass Units (IGU) | Structural sealants for IGU edge seals in structural glazing applications |
| Panel Bonding | Structural adhesion of architectural panels (metal, composite, ceramic) to supporting frameworks |
| Glass Embedding | Structural glass fins, glass beams, and embedded glass connections |
| Silicone Sealant Manufacturing | R&D, QC, and technical data sheet generation for structural silicone products |
| Third-Party Testing & Certification | Independent verification for building code compliance and product approvals |
| Facade Engineering | Design validation and material selection for structurally glazed façades |
| Specification Compliance | Meeting ASTM C1406 and other structural glazing specifications that reference C1135 |
Related Stadard:
| ISO 8339 | Building construction - Sealants - Determination of tensile properties (Extension to break) |
| ASTM C1135 | Standard Test Method for Determining Tensile Adhesion Properties of Structural Sealants |
| ISO 8340 | Building construction - Sealants - Determination of tensile properties at maintained extension |
| ISO 7389 | Building construction - Jointing products - Determination of elastic recovery of sealants |
| GB/T 13477.8 | Test method for building sealants—Part 8:Determination of tensile properties |
| ISO 10590 | Building Construction Sealants Determination of Tensile Properties of Sealants at Maintained Extension After Immersion in Water |
| ISO 19862 | Buildings and civil engineering works — Sealants — Durability to extension compression cycling under accelerated weathering |
| ASTM C719 | Standard Test Method for Adhesion and Cohesion of Elastomeric Joint Sealants Under Cyclic Movement (Hockman Cycle) |
Keywords: UnitedTest ASTM C1135 tester, ASTM C1135 structural sealant tensile adhesion tester, structural glazing sealant tensile test machine, rigid substrate sealant tensile strength testing equipment, ASTM C1135 glass metal framing structural sealant tensile adhesion test, structural glazing joint tensile stress elongation analyzer, ultimate tensile strength and failure mode test for architectural sealants, rigid panel bonded structural sealant laboratory tester, curtain wall structural sealant
Related products and device
Related Standard
ISO 8339 Building construction — Sealants — Determination of tensile properties (Extension to break)
ISO 8339 defines a laboratory tensile test method to measure full tensile mechanical performance of construction joint sealants by stretching bonded specimens until complete rupture. It quantifies secant modulus and elongation-at-break, which are core material parameters to evaluate elastic deformability and adhesion/cohesion of sealants under tension. It focuses on single-rate tensile extension to full failure, distinct from ISO 8340 which tests sustained constant tensile loading.
ASTM D1002 is the most widely used standard test for measuring the apparent shear strength of metal‑to‑metal adhesive single‑lap joints under tension loading. It provides comparative data for adhesive selection, process control, and quality assurance in structural bonding applications. It is the most common test for evaluating adhesive shear performance.
ASTM D897 prescribed a method for determining the comparative tensile properties of adhesive bonds in a standard specimen when tested under specific conditions. Its primary purpose was to measure the tensile strength of an adhesive bond between two rigid substrates (metal to metal).
FAQs for ASTM C1135 Tensile Adhesion Test for Structural Sealants
Q1: What is the primary purpose of ASTM C1135?
A1: ASTM C1135 measures tensile adhesion strength, graded tensile stress at defined elongations (10%, 25%, 50%, 100%), ultimate elongation, and failure mode percentage for structural glazing sealants (mainly structural silicones). It generates lab data to evaluate if a sealant meets US curtain wall, structural glazing and AAMA building code requirements.
Q2: What products does this standard apply to, and what is excluded?
A2: Scope covers load-bearing structural sealants that bond glass to metal framing for curtain walls, insulated glass units, and facade panels. It excludes non-structural weather caulks, consumer sealants, and industrial non-construction adhesives.
Q3: What are the two referenced ISO standards similar to ASTM C1135?
A3: ISO 8339 (tensile extension to break for building sealants) and ISO 8340 (tensile test under sustained constant extension for creep evaluation). ASTM C1135 follows different specimen geometry, speed and conditioning rules than both ISO standards.
Q4: What is a structural sealant as defined in ASTM C717?
A4: A sealant designed to transfer permanent structural tensile loads between glass panels and metal framing, resisting wind pressure, thermal movement and dead weight of glazing assemblies.
Q5: What is the standard sealant cavity dimension for test specimens?
A5: Fixed cavity size: 12.7 mm width × 12.7 mm thickness × 50.8 mm length, formed with a single-piece PTFE non-stick spacer between two glass substrates.
Q6: What is the standard substrate material and size?
A6: Standard substrate is clear float glass with dimensions 6.3 mm (thick) × 25.4 mm (wide) × 76.2 mm (long). Aluminium or other rigid substrates can be used but must be documented for comparison.
Q7: How many replicate specimens are required for one sealant/substrate combination?
A7: Minimum of 5 identical specimens for baseline room-temperature testing. An additional set of 5 specimens is required for every supplementary ageing treatment (7-day water immersion, thermal cycling, cold exposure).
Q8: What is the mandatory cure time before testing?
A8: Specimens must cure for 21 full days under standard laboratory ambient conditions before spacer removal and tensile testing. If spacers are removed early, this deviation must be fully noted in the test report.
Q9: What cleaning solution is recommended for glass substrates?
A9: A 50/50 mixture of isopropanol and water with lint-free cloths, wiped while the surface is still damp to eliminate surface contaminants that harm adhesion.
Q10: What is edge bite (Dimension B) and why do we measure it?
A10: Edge bite (B) is the width of the contact zone between sealant and glass substrate. Together with bond length (A), it calculates the actual bonded contact area D = A × B, which is used to compute accurate tensile stress values.
Test Equipment & Test Parameter FAQs
Q11: What mandatory crosshead speed is specified for tensile testing?
A11: Fixed pull rate of 50.8 mm/min (2.0 in/min), with a tolerance of ±5.1 mm/min. Chart recorder speed minimum: 127 mm/min (5.0 in/min); 508 mm/min is preferred for precise strain readings.
Q12: What special grip design is required for the tensile machine?
A12: Self-aligning swivel/universal joint grips are mandatory to avoid eccentric side loading that creates artificial peel stress and skews tensile strength results. Grips clamp only the glass substrate ends, never touch the sealant zone.
Q13: What material must the spacer be made of?
A13: Solid PTFE (Teflon) or other rigid non-adherent material so the cured sealant does not stick to the spacer during moulding.
Q14: What elongation points must force data be recorded at?
A14: Tensile load values must be captured at 10%, 25%, 50%, 100% strain, plus the peak ultimate load at specimen rupture.
Q15: How to calculate tensile stress per ASTM C1135 formulas?
A15: Actual contact area D = Bond length (A) × Edge bite (B)
Tensile Stress T = Measured load C ÷ Contact area D
Units: N/mm² (MPa) or lbf/in² (psi)
Q16: What counts as valid vs invalid test data when glass breaks?
A16: If the glass substrate fractures before sealant rupture, all load values recorded before substrate breakage are still usable; only the ultimate rupture load at glass failure is discarded.
Q17: How to classify and report failure mode?
A17: Visually inspect the fractured sealant surface and record the percentage of cohesive failure (crack inside sealant bulk). High cohesive percentage (>90%) indicates reliable structural adhesion; full adhesive failure means poor bonding to glass.
Q18: Does ASTM C1135 provide official precision data?
A18: Yes, interlaboratory repeatability (Kr) and reproducibility (KR) values are published for tensile stress at each elongation, ultimate strength, ultimate elongation and cohesive failure percentage, based on round-robin testing of acid and neutral structural silicones.
Q19: What's the Key difference of ASTM C1135 vs. ISO 8339?
| Feature | ASTM C1135 | ISO 8339 |
|---|---|---|
| Specimen geometry | H-shaped, 12.7 × 12.7 × 50.8 mm cavity | H-shaped, 12 × 12 × 50 mm cavity |
| Default substrate | Clear float glass (6.3 × 25.4 × 76.2 mm) | Mortar, anodized aluminium, or glass (per ISO 13640) |
| Extension rate | 50.8 mm/min (2.0 in./min) | 5 mm/min (5.5 ± 0.7 mm/min) |
| Test temperatures | Standard conditions (23°C ± 2°C, 50% ± 5% RH) | 23°C and −20°C |
| Data recorded | Tensile stress at 10%, 25%, 50%, 100% strain + peak | Secant modulus at chosen elongation + elongation at break |
| Curing | 21 days standard conditions | 28 days (Method A) or heat/water cycled (Method B) |
| Output | Tensile stress vs. strain; cohesive failure % | Secant modulus; elongation at break |
| Application focus | Structural sealants (glazing/panel to frame) | General building construction sealants |
Q20: What is the difference between ASTM C1135 and ASTM C794?
A20: ASTM C1135 is uniaxial tensile test for load-bearing structural sealants. ASTM C794 is a peel adhesion test for non-structural weather sealants and cannot be used for structural glazing qualification.
Q21: What AAMA specification references ASTM C1135?
A21: AAMA 1105 (North American structural silicone sealant performance standard) mandates ASTM C1135 tensile data as a core compliance requirement for facade product certification.
Q22: Why is ASTM C1135 a critical test for structural silicone sealants?
A22: US Regulatory Compliance: Mandatory test method for AAMA certification and US building code approval for structural curtain wall glazing. Without C1135 test data, sealants cannot be specified for load-bearing glass-to-metal bonding.
Engineering Design Data: Tensile stress at 10/25/50/100% elongation provides exact material parameters for architects to calculate wind, thermal and dead load stress on facade assemblies.
Adhesion Reliability Indicator: Cohesive failure percentage quantifies bonding quality; adhesive failure signals defective surface cleaning or incompatible primer/substrate pairs.
Standardized QC for Mass Production: Factory batch testing filters low-performance sealant batches before facade installation, preventing costly water leakage or glass drop failures.
Water Resistance Validation: Paired with 7-day water immersion pre-treatment, it evaluates sealant tensile retention after rain exposure for exterior facades.
Interlab Comparability: Published repeatability/reproducibility data ensures consistent results between manufacturers, third-party labs and curtain wall fabricators across North America.
Differentiate structural vs non-structural caulks: Distinguishes load-bearing structural silicones from decorative non-load joint sealants via ultimate tensile capacity metrics.
Q23: Which industrial sectors rely on ASTM C1135 testing?
A23: Curtain wall and architectural facade manufacturing
Structural silicone sealant production & R&D laboratories
Insulated glass (IG) unit manufacturers
Third-party US construction material certification labs
Commercial building design & structural engineering firms
AAMA product certification bodies
Window and glazing fabrication factories
Q24: What are the main limitations of ASTM C1135?
A24: No mandatory low-temperature (-20°C) tensile testing, so cold brittleness risk requires separate custom cold chamber testing.
Optimized for float glass substrates; test results cannot be directly extrapolated to aluminium, steel or composite panels without dedicated specimen sets.
Only static single-stretch tensile testing; it does not simulate cyclic wind fatigue loads on facades.
Does not measure long-term creep under sustained tension (needs supplementary creep testing such as ISO 8340).
Fixed 21-day ambient cure standard; no standardized accelerated heat curing procedure within the method.
Test Report & Compliance FAQs
Q25: How does ASTM C1135 relate to real-world structural glazing design?
A25: In a curtain wall, the structural silicone sealant must:
Carry the dead load of the glass lite (weight hanging from the top edge)
Resist wind loads (both positive and negative pressure)
Accommodate thermal and structural movement (joint stretching and compression)
Maintain adhesion for decades under environmental exposure
ASTM C1135 measures the sealant's tensile adhesion capacity under controlled laboratory conditions that mimic the actual joint geometry (H-shaped specimen with two substrate/sealant interfaces loaded in pure tension). The data is directly translatable to design calculations — engineers can determine if the sealant can support the glass weight at the design joint depth, and establish appropriate safety factors.
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