Information on the most widely used ASTM standards within the materials testing industry
ISO 10468 GRP Pipe Ring Creep Properties Tester | Wet & Dry Condition Test | UnitedTest
UnitedTest manufactures high-performance ISO 10468 compliant GRP pipe ring creep test machines, engineered to evaluate long-term time-dependent mechanical properties of glass-reinforced thermosetting plastics (GRP) pipes under both dry and wet environmental conditions.
ISO 10468 Glass-reinforced thermosetting plastics (GRP) pipes — Determination of the ring creep properties under wet or dry conditions is a key international standard focusing on long-term structural performance testing of GRP pipelines. It quantifies two critical time-dependent mechanical indicators: long-term ring creep stiffness and creep factor, which are essential for assessing the durability and structural stability of GRP pipes over extended service periods.
The standard defines two distinct testing environments to meet diverse industrial evaluation needs. Thedry creep test is primarily used for raw material batch consistency verification and factory internal quality control, ensuring uniform mechanical performance of GRP pipe raw materials. The wet creep test simulates real underground water immersion service conditions, enabling accurate prediction of long-term structural performance and service reliability for buried GRP pipes in underground engineering applications.
Our professional ISO 10468 testing equipment delivers stable, repeatable creep property test data, supporting GRP pipe material R&D, production quality inspection, and long-term service life assessment for municipal and industrial pipeline projects.
Test Principle
A short ring-shaped GRP pipe specimen is horizontally mounted and subjected to a constant vertical diametral compressive load over thousands of hours. The vertical diameter deflection is periodically recorded at logarithmic time intervals.
First, calculate the target load to induce controlled initial wall strain (0.13%–0.17%) within 3 minutes after loading, per second-order deflection theory.
Maintain constant force throughout the test while measuring time-dependent vertical deflection.
Convert deflection readings into time-series ring stiffness values using the deflection coefficient formula.
Apply regression extrapolation (ISO 10928 Method B) to derive long-term creep stiffness at a specified design time point (e.g., 50 years, 100 years).
Compute creep factor as the ratio of long-term creep stiffness to initial ring stiffness measured at 0.1 h on the same specimen; the final declared creep factor is the average of two replicate specimens.
Specific Test Method (Two Parallel Test Modes)
Method A: Dry Ring Creep Test
No water immersion; test assembly operates under ambient conditioned air.
Main use: Raw resin, glass fiber and laminate formulation consistency verification, factory incoming material QC.
No water tank required; all loading and measuring devices exposed to air.
Method B: Wet Ring Creep Test
Specimen fully submerged in pH 7 tap water at specified constant test temperature.
Main use: Simulate sewer, drainage, underground water pipeline service conditions to assess water-induced creep degradation of GRP composite.
Buoyancy of submerged specimen must be offset when calculating applied vertical compressive force F.
Minimum test duration for wet creep modulus determination exceeds 10,000 hours.
Two Loading Sub-methods (Selectable)
Flat bearing plate loading: Plates cover full specimen length, minimum width 100 mm.
Beam bar loading: Flat contact face width 15–55 mm; sharp edges forbidden.
Hybrid loading (one plate + one beam bar, axes perpendicular) is also permitted.
Testing Equipment for ISO 10468 GRP Pipe Ring Creep Test:
| Compressive Loading Machine | Capable of stable constant vertical compressive force application with calibrated load accuracy within ±1% of applied force value. Dead-weight loading systems are acceptable. |
| Force Application Surfaces | Bearing plates: Rigid, flat, smooth, parallel, length ≥ specimen length, width ≥100 mm, no visible bending under test load.
Beam bars: Rigid, full-length flat contact surface 15–55 mm wide; non-contact structural parts must not touch specimen.
|
| Water Container (Only for Wet Testing) | Large enough to fully submerge the loaded ring specimen; holds pH 7 tap water with stable constant temperature and fixed water level to eliminate buoyancy fluctuation interference on applied load. |
| Auxiliary Supplies | Reference marking pens (draw 60° interval longitudinal reference lines on pipe inner/outer wall), optional end-sealing material for specimen cut ends. |
Test Specimen Information
Specimen form: Complete circular pipe ring cut from production GRP pipe.
Required quantity: Minimum 2 identical ring specimens for each test condition (wet/dry).
Specimen length L: Default (300 ±15) mm if no specification in product referencing standard; tolerance ±5% when specified.
Cutting requirements: Cut ends smooth, perpendicular to pipe central axis; ends may be sealed to prevent water penetration into laminate for wet testing.
Marking rule: Draw longitudinal reference lines every 60° around circumference; one pair of diametrically opposite lines defined as "Position 1" (the measuring reference location for stiffness calculation).
Test Parameter & Stipulations
Initial strain target: Calculated surface strain at pipe crown/invert controlled between 0.13% and 0.17% at 3 min post-loading.
Loading completion time: Target deflection must be reached within 3 minutes after force application.
Load maintenance: Vertical compressive force F kept constant for full test duration.
Deflection reading schedule: Start sampling no later than 1 h after loading; collect ~10 evenly spaced data points per decade of log(time) over logarithmic time intervals; record deflection precision within ±2% of initial deflection.
Extrapolation timeline: Standard extrapolation target time (e.g., 50 years, 100 years) defined by product design standard; wet test minimum run time >10,000 hours.
Water condition (wet test only): Tap water pH = 7, fixed constant test temperature specified by referencing standard.
Specimen alignment: Position 1 reference lines must be vertically aligned under compressive force; plates/beam bars cannot tilt sideways, contact between specimen and loading surfaces must be uniform.
Rigidity requirement: Plates and beam bars must not deform visibly during loading.
Standardized Full Test Procedures of ISO 10468 GRP Pipe Ring Creep Test:
Measure and record all specimen dimensions per ISO 3126.
Measure initial ring stiffness S₀,₁ at Position 1 following ISO 7685; compute the target vertical force F to generate 0.13%–0.17% initial strain within 3 min.
Mount ring specimen onto loading apparatus, align Position 1 vertically; install water tank and submerge specimen fully if performing wet creep test, stabilize water level and temperature.
Apply calculated constant vertical force F within 3 min, record actual applied force and achieved initial deflection.
Maintain constant load continuously; take deflection readings at logarithmic time intervals starting at ≤1 h post-loading, record all time-deflection data.
After test duration ends, process data: calculate ring creep stiffness Sₓ,₁,creep for each time point using deflection coefficient formula.
Conduct regression analysis via ISO 10928 Method B to extrapolate long-term ring creep stiffness at design service life x years.
Calculate single-specimen creep factor αₓ,creep, then average results from two specimens as the official creep factor.
Compile complete test report.
Related Test Standard:
| ISO 10468 | Glass-reinforced thermosetting plastics (GRP) pipes - Determination of the ring creep properties under wet or dry conditions |
| GOST R 57006 | Fiberglass-reinforced thermosetting plastic pipes and parts of pipelines. Test method for long-term specific ring creep stiffness and wet creep factor under wet conditions |
| ISO 7685 | Glass-reinforced thermosetting plastics (GRP) pipes — Determination of initial ring stiffness |
| ISO 15306 | Glass-reinforced thermosetting plastics (GRP) pipes - Determination of the resistance to cyclic internal pressure |
Industry Applications
This standard exclusively serves GRP (fiberglass reinforced thermoset plastic) piping industry, covering:
Municipal underground gravity sewer and drainage pipelines (primary wet creep test application).
Potable water, industrial process liquid non-pressure GRP pipelines.
Civil engineering trenchless buried composite pipelines, tunnel drainage liners.
Factory quality control of raw GRP laminate materials, pipe formulation development, batch consistency inspection (dry creep test).
Third-party product certification, pipeline structural design verification, compliance testing for national/international GRP pipe product standards.
R&D of new GRP composite formulations with enhanced long-term anti-creep performance for underground water-bearing environments.
Keywords: UnitedTest ISO 10468 tester, ISO 10468 GRP pipe ring creep tester, wet dry condition GRP pipe creep test machine, GRP pipe long-term structural performance tester, ISO 10468 ring creep stiffness and creep factor test, water immersed GRP pipe long-term creep testing, buried GRP pipe underground service performance test, dry condition GRP pipe batch quality control tester, time-dependent mechanical property test for thermosetting plastic pipes
Related products and device
Related Standard
ASTM D2412: Standard Test Method for Determination of External Loading Characteristics of Plastic Pipe by Parallel-Plate Loading
Plastic pipe compression test, or pipe ring stiffness tseter is a testing standard used to determine the stiffness and load deflection of plastic pipe. This summary is intended to help you understand the basic procedure and equipment required to complete this test with accuracy.
ASTM D2412 test method covers the determination of load-deflection characteristics of plastic pipe under parallel-plate loading.
ISO 9967:2016 Thermoplastics pipes — Determination of creep ratio
This standard specifies a method for determining the creep ratio of thermoplastics pipes having a circular cross-section.
The ISO 9967 test procedure begins by preparing a ring-shaped specimen from a thermoplastic pipe. The ring is typically cut to a length equal to the pipe's outer diameter and must be free of visible defects. Before testing, the sample is conditioned, usually at 23°C for at least 24 hours. During the test, the specimen is placed vertically between two flat, parallel plates in a compression testing machine. A constant external force is applied to the ring to compress it until a deformation equal to 3% of its mean diameter is reached. This loading should occur gradually, typically within one minute. The test apparatus must maintain this compressive load over an extended period, most commonly 10,000 hours, under controlled environmental conditions. The deformation of the ring is measured at defined intervals during the test using a precise displacement measurement device. Initial and long-term measurements are used to calculate the creep ratio. This ratio quantifies how much the ring deforms over time under constant load, which indicates the material's long-term behavior and suitability for buried, non-pressure pipe applications. Accurate time tracking and temperature control are critical throughout the process to ensure valid results. The test concludes by comparing the deformation at 30 minutes and at the final time point to calculate the creep ratio according to the formula provided in the ISO 9967 standard.
ISO 8521 Glass-reinforced thermosetting plastic (GRP) pipes — Test methods for the determination of the initial circumferential tensile wall strength
ISO 8521 specifies six test methods (A, B, C, D, E, F) to determine the initial circumferential tensile wall strength per unit length of GRP pipes — a property also commonly called "hoop tensile strength." Both terms are interchangeable per the standard . The result is expressed in newtons per millimetre (N/mm) of circumference. "Initial" means the strength at the startof loading (short-term / instantaneous), as opposed to long-term hydrostatic strength covered by other standards.
Frequently Asked Questions (FAQs) — ISO 10468 Ring Creep Test for GRP Pipes
Q1: What is ISO 10468:2023 used to test?
A1: It defines uniform lab test methods to measure ring creep stiffness and creep factor of GRP (glass-reinforced thermosetting plastic) pipes. Tests can run under fully water-immersed wet conditions or dry ambient conditions to evaluate time-dependent deformation under constant external compression.
Q2: Why is ISO 10468 creep testing mandatory for GRP pipes instead of just doing ISO 7685 short-term ring stiffness?
A2: GRP is a viscoelastic composite material. Short-term ring stiffness (ISO 7685, measured at 0.1 h) only reflects instantaneous rigidity. Under sustained soil pressure underground, GRP slowly deforms over decades (creep). ISO 10468 captures this time-dependent softening and extrapolates long-term stiffness; without this data, engineers cannot calculate safe wall thickness or predict pipe ovalization risk over 50/100-year design life.
Q3: Why is the ISO 10468 ring creep test important for GRP pipes?
A3: GRP (glass-reinforced thermosetting plastic) is a viscoelastic composite material — it continues to deform slowly under a sustained load over time. A short-term stiffness measurement (like initial ring stiffness per ISO 7685) cannot predict how the pipe will behave after 10, 20, or 50 years of burial under soil and traffic loads. ISO 10468 provides a standardized, reproducible method to:
Quantify long-term ring creep stiffness (Sₓ,₁,creep)
Determine the creep factor (αₓ,creep)
Enable safe structural design (deflection limits, wall thickness optimization)
Support material qualification, quality control, and regulatory compliance
Without this test, engineers would have no reliable data to guarantee the pipe won't exceed allowable deflection (typically 5% of diameter) over its design life.
Q4: What is the difference between "dry" and "wet" creep testing?
| Aspect | Dry Creep Test | Wet Creep Test |
|---|---|---|
| Environment | Air (ambient or conditioned) | Full immersion in tap water (pH 7 ± 2) |
| Purpose | Assessment & control of raw material consistency | Determination of long-term creep performance in simulated service (buried/underwater) conditions |
| Duration | Typically shorter | > 10,000 h (to enable extrapolation to decades) |
| Frequency | Routine QC / batch verification | Design qualification / product certification |
Q5: What is a creep factor, and why is it the core output of this test?
A5: Creep factor is the ratio of long-term extrapolated ring creep stiffness to the initial 0.1 h ring stiffness of the same specimen. It quantifies how much the pipe’s rigidity declines over service time. Pipeline design standards use this factor to reduce short-term stiffness values for long-term structural safety calculations. The final reported value must be the average of two test pieces.
Q6: Why perform wet creep testing separately from dry creep?
A6: Water penetrates the GRP laminate and weakens the resin-fiber bonding interface, accelerating creep deformation significantly. Dry test results cannot represent real buried sewer/water pipe service environments. Wet creep reproduces water immersion ageing to measure actual long-term deformation risk in underground water-bearing soils.
Q7: How many pipe ring specimens are required for one complete ISO 10468 test batch?
A7: A minimum of two identical full ring specimens, tested under identical wet/dry conditions. Creep factor is averaged from the two results; single-specimen data is not acceptable for official compliance reports.
Q8: What is the standard length of test specimens?
A8: If no product standard specifies length, the specimen ring length shall be (300 ±15) mm. If a referencing standard defines a custom length, a ±5% tolerance is allowed. Cut ends must be smooth and perpendicular to the pipe axis and can be sealed to stop water ingress during wet testing.
Q9: Why mark longitudinal reference lines every 60° around the pipe circumference?
A9: One pair of diametrically opposite lines is designated “Position 1”, the fixed location for measuring deflection and calculating ring stiffness throughout the test. Equal 60° spacing ensures uniform reference positioning and avoids measurement bias from uneven pipe wall structure.
Q10: What two loading contact systems are permitted in ISO 10468?
A10: Bearing flat plates: Min width 100 mm, length matching specimen length, rigid with no bending under load;
Beam bars: Flat contact surface width 15–55 mm, full length, no sharp edges.
A hybrid setup (one plate + one beam bar with perpendicular axes) is also allowed.
Q11: What requirements does the water tank for wet creep testing need to meet?
A11: It must fully submerge the loaded ring specimen, hold pH 7 tap water, maintain constant specified test temperature, and keep a stable water level to eliminate buoyancy interference on the constant compressive load.
Q12: What target initial strain do we need to achieve within 3 minutes of loading?
A12: The calculated inner surface strain at pipe crown and invert (Position 1) must be controlled between 0.13% and 0.17% when load is fully applied within 3 minutes. This standardized strain level ensures consistent comparative creep data across all labs.
Q13: How do we process raw deflection data to get long-term creep stiffness?
A13: Calculate real-time ring creep stiffness using the deflection coefficient formula for each time point;
Use regression analysis Method B defined in ISO 10928:2016 to fit stiffness-time data;
Extrapolate the fitted curve to the design service life (e.g., 50 years, 100 years) specified by the product standard to get long-term ring creep stiffness.
Q14: What risks could occur if manufacturers skip ISO 10468 creep testing for buried GRP pipes?
A14: Engineers will lack valid long-term stiffness data, leading to under-designed pipe wall thickness;
Excessive long-term ovalization under soil load, causing joint separation, sewage leakage, or complete pipe collapse;
Water-induced accelerated creep unquantified, leading to premature infrastructure failure decades before design service life;
Non-compliance with municipal pipeline regulatory standards, invalidating product certification and construction approval.
Q15: What happens if the force fluctuates during the test?
A15: The standard requires the force to be maintained constant within ±1% of the applied value for the entire duration. Fluctuations invalidate the data because creep deflection is force-dependent. For wet tests, buoyancy effects from water level changes and the mass of the upper platen/beam bar must be accounted for. Modern servo-controlled hydraulic or electromechanical machines with closed-loop feedback are typically used.
Q16: What are common reasons for test invalidation?
A16: Incorrect specimen length (outside ±5% tolerance)
Misaligned reference lines (position 1 not vertical)
Tilted plates/beam bars causing uneven contact
Force not reaching target deflection within 3 min
Insufficient number of data points (< 10 per log decade)
Water pH drifting outside 7 ± 2 during wet test
Using different loading arrangements for initial vs. long-term measurement
Buoyancy not compensated in wet test
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